ET Aqueous Colloids Research Group
Techniques and available methods
Materials synthesis: synthesis of nanoparticles: coprecipitation of Fe(II) and Fe(III) ions in alkaline medium, YIG
(yttrium-iron oxide garnet) self-combustion of ruby jelly, Stöeber method, hydrothermal ageing, etc.
Equipments for preparation: water purification system, mixers, heating baskets, thermal baths, supercentrifuge
(Sorwall), driers, ovens, furnaces (up to 1300oC), freeze-drier, high energy ultrasonication and colloidal mill
(vibrating agate mill), pH-meter, conductivity meter.
Surface modification: design and implementation of organic shell on core
for example magnetite nanoparticles by adsorption of surfactants, polyacids, natural and synthetised
polyelectrolytes/polymers to stabilize and functionalize them for further functionalization (e.g. by anti-body)
Characterization: of interfacial equilibria and colloidal interactions
mainly pH and ionic strength dependent properties tuned by surface modifying agents
pH-dependent charge state of particles and molecules (Potentiometric acid-base titration system)
Particle size and size distribution, coagulatoin kinetics by dynamic light scattering (NanoZS and Zetasizer4)
Charge state of particles by laser Doppler electrophoresis (NanoZS)
2-D interactions in floating films by Langmuir-balance (MicroTroughXL)
Flow properties of materials, flow curves, creep tests, oscillation measurements, etc. (RS150 rheometer)
Magnetic measurements, particle separation by size using various magnetic field strengths (Hall-probe,
Separator)
UV-visible optical properties of materials (dioda array spectrophotometer)
Magnetic hyperthermia simulation (Magnetherm)
Advanced methods (XRD, TEM, SEM) for further characterization of nanoparticles are available at our University.
Contact:
ET Aqueous Colloids
Research Group
HU-6720 Szeged
Aradi Vt. tere 1.
E-mail: tombacz@
chem.u-szeged.hu
Phone: +36-62/544212